7: Technique Summaries
- Page ID
- 93161
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\(\newcommand{\avec}{\mathbf a}\) \(\newcommand{\bvec}{\mathbf b}\) \(\newcommand{\cvec}{\mathbf c}\) \(\newcommand{\dvec}{\mathbf d}\) \(\newcommand{\dtil}{\widetilde{\mathbf d}}\) \(\newcommand{\evec}{\mathbf e}\) \(\newcommand{\fvec}{\mathbf f}\) \(\newcommand{\nvec}{\mathbf n}\) \(\newcommand{\pvec}{\mathbf p}\) \(\newcommand{\qvec}{\mathbf q}\) \(\newcommand{\svec}{\mathbf s}\) \(\newcommand{\tvec}{\mathbf t}\) \(\newcommand{\uvec}{\mathbf u}\) \(\newcommand{\vvec}{\mathbf v}\) \(\newcommand{\wvec}{\mathbf w}\) \(\newcommand{\xvec}{\mathbf x}\) \(\newcommand{\yvec}{\mathbf y}\) \(\newcommand{\zvec}{\mathbf z}\) \(\newcommand{\rvec}{\mathbf r}\) \(\newcommand{\mvec}{\mathbf m}\) \(\newcommand{\zerovec}{\mathbf 0}\) \(\newcommand{\onevec}{\mathbf 1}\) \(\newcommand{\real}{\mathbb R}\) \(\newcommand{\twovec}[2]{\left[\begin{array}{r}#1 \\ #2 \end{array}\right]}\) \(\newcommand{\ctwovec}[2]{\left[\begin{array}{c}#1 \\ #2 \end{array}\right]}\) \(\newcommand{\threevec}[3]{\left[\begin{array}{r}#1 \\ #2 \\ #3 \end{array}\right]}\) \(\newcommand{\cthreevec}[3]{\left[\begin{array}{c}#1 \\ #2 \\ #3 \end{array}\right]}\) \(\newcommand{\fourvec}[4]{\left[\begin{array}{r}#1 \\ #2 \\ #3 \\ #4 \end{array}\right]}\) \(\newcommand{\cfourvec}[4]{\left[\begin{array}{c}#1 \\ #2 \\ #3 \\ #4 \end{array}\right]}\) \(\newcommand{\fivevec}[5]{\left[\begin{array}{r}#1 \\ #2 \\ #3 \\ #4 \\ #5 \\ \end{array}\right]}\) \(\newcommand{\cfivevec}[5]{\left[\begin{array}{c}#1 \\ #2 \\ #3 \\ #4 \\ #5 \\ \end{array}\right]}\) \(\newcommand{\mattwo}[4]{\left[\begin{array}{rr}#1 \amp #2 \\ #3 \amp #4 \\ \end{array}\right]}\) \(\newcommand{\laspan}[1]{\text{Span}\{#1\}}\) \(\newcommand{\bcal}{\cal B}\) \(\newcommand{\ccal}{\cal C}\) \(\newcommand{\scal}{\cal S}\) \(\newcommand{\wcal}{\cal W}\) \(\newcommand{\ecal}{\cal E}\) \(\newcommand{\coords}[2]{\left\{#1\right\}_{#2}}\) \(\newcommand{\gray}[1]{\color{gray}{#1}}\) \(\newcommand{\lgray}[1]{\color{lightgray}{#1}}\) \(\newcommand{\rank}{\operatorname{rank}}\) \(\newcommand{\row}{\text{Row}}\) \(\newcommand{\col}{\text{Col}}\) \(\renewcommand{\row}{\text{Row}}\) \(\newcommand{\nul}{\text{Nul}}\) \(\newcommand{\var}{\text{Var}}\) \(\newcommand{\corr}{\text{corr}}\) \(\newcommand{\len}[1]{\left|#1\right|}\) \(\newcommand{\bbar}{\overline{\bvec}}\) \(\newcommand{\bhat}{\widehat{\bvec}}\) \(\newcommand{\bperp}{\bvec^\perp}\) \(\newcommand{\xhat}{\widehat{\xvec}}\) \(\newcommand{\vhat}{\widehat{\vvec}}\) \(\newcommand{\uhat}{\widehat{\uvec}}\) \(\newcommand{\what}{\widehat{\wvec}}\) \(\newcommand{\Sighat}{\widehat{\Sigma}}\) \(\newcommand{\lt}{<}\) \(\newcommand{\gt}{>}\) \(\newcommand{\amp}{&}\) \(\definecolor{fillinmathshade}{gray}{0.9}\)The following summary sheets are not intended as a substitute for reading the sections on each technique. The purpose of these summary sheets is to review the main points for students who have already read the sections. They can also be useful for students who have previously performed these techniques (earlier in a semester or in recent years) and wish to remind themselves about minor details
- 7.1: Flame-Drying Glassware
- Procedural summary for flame drying glassware.
- 7.2: Using Calibrated Glass Pipettes
- Procedural summary for using calibrated glass pipettes.
- 7.3: Inert Atmospheric Methods
- Procedural summary for inert atmospheric methods.
- 7.4: Reflux
- Procedural summary for reflux.
- 7.5: Suction Filtration
- Procedural summary for suction filtration (vacuum filtration).
- 7.6: Hot Filtration
- Procedural summary for hot filtration.
- 7.7: Thin Layer Chromatography
- Procedural summary for thin layer chromatography.
- 7.8: TLC Visualization Methods
- Procedural summary for TLC visualization methods.
- 7.9: Macroscale Column Chromatography
- Procedural summary for macroscale column chromatography.
- 7.10: Pipette Column Chromatography
- Procedural summary for pipette column chromatography.
- 7.11: Testing Solvents for Crystallization
- Procedural summary for testing solvents for crystallization.
- 7.12: Testing Mixed Solvents for Crystallization
- Procedural summary for testing mixed solvents for crystallization.
- 7.13: Single Solvent Crystallization
- Procedural summary for single solvent crystallization.
- 7.14: Mixed Solvent Crystallization
- Procedural summary for mixed solvent crystallization.
- 7.15: Single Extraction
- Procedural summary for single extraction.
- 7.16: Multiple Extraction
- Multiple extraction flow-chart when the organic layer is on the top or when the aqueous layer is on the top.
- 7.17: Microscale Extractions
- Procedural summary for microscale extractions.
- 7.18: Testing the pH After a Wash
- Procedural summary for testing the pH after a wash.
- 7.19: Using Drying Agents
- Procedural summary for using drying agents.
- 7.20: Acid-Base Extraction
- Flow-charts for acid-base extraction.
- 7.21: Simple Distillation
- Procedural summary for simple distillation.
- 7.22: Fractional Distillation
- Procedural summary for fractional distillation.
- 7.23: Vacuum Distillation
- Procedural summary for vacuum distillation.
- 7.24: Steam Distillation
- Procedural summary for Steam Distillation
- 7.25: Rotary Evaporation
- Procedural summary for rotary evaporation.
- 7.26: Melting Points
- Procedural summary for obtaining a melting point.
- 7.27: Boiling Points (Thiele Tube)
- Procedural summary for obtaining a boiling point.
- 7.28: Vacuum Sublimation
- Procedural summary for vacuum sublimation.