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7: Technique Summaries

Last updated

Apr 7, 2022
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- 6.4D: Individual Tests
- 7.1: Flame-Drying Glassware

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The following summary sheets are not intended as a substitute for reading the sections on each technique. The purpose of these summary sheets is to review the main points for students who have already read the sections. They can also be useful for students who have previously performed these techniques (earlier in a semester or in recent years) and wish to remind themselves about minor details

7.1: Flame-Drying Glassware
Procedural summary for flame drying glassware.
7.2: Using Calibrated Glass Pipettes
Procedural summary for using calibrated glass pipettes.
7.3: Inert Atmospheric Methods
Procedural summary for inert atmospheric methods.
7.4: Reflux
Procedural summary for reflux.
7.5: Suction Filtration
Procedural summary for suction filtration (vacuum filtration).
7.6: Hot Filtration
Procedural summary for hot filtration.
7.7: Thin Layer Chromatography
Procedural summary for thin layer chromatography.
7.8: TLC Visualization Methods
Procedural summary for TLC visualization methods.
7.9: Macroscale Column Chromatography
Procedural summary for macroscale column chromatography.
7.10: Pipette Column Chromatography
Procedural summary for pipette column chromatography.
7.11: Testing Solvents for Crystallization
Procedural summary for testing solvents for crystallization.
7.12: Testing Mixed Solvents for Crystallization
Procedural summary for testing mixed solvents for crystallization.
7.13: Single Solvent Crystallization
Procedural summary for single solvent crystallization.
7.14: Mixed Solvent Crystallization
Procedural summary for mixed solvent crystallization.
7.15: Single Extraction
Procedural summary for single extraction.
7.16: Multiple Extraction
Multiple extraction flow-chart when the organic layer is on the top or when the aqueous layer is on the top.
7.17: Microscale Extractions
Procedural summary for microscale extractions.
7.18: Testing the pH After a Wash
Procedural summary for testing the pH after a wash.
7.19: Using Drying Agents
Procedural summary for using drying agents.
7.20: Acid-Base Extraction
Flow-charts for acid-base extraction.
7.21: Simple Distillation
Procedural summary for simple distillation.
7.22: Fractional Distillation
Procedural summary for fractional distillation.
7.23: Vacuum Distillation
Procedural summary for vacuum distillation.
7.24: Steam Distillation
Procedural summary for Steam Distillation
7.25: Rotary Evaporation
Procedural summary for rotary evaporation.
7.26: Melting Points
Procedural summary for obtaining a melting point.
7.27: Boiling Points (Thiele Tube)
Procedural summary for obtaining a boiling point.
7.28: Vacuum Sublimation
Procedural summary for vacuum sublimation.

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