8.6: Additional Resources
- Page ID
- 163753
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\(\newcommand{\avec}{\mathbf a}\) \(\newcommand{\bvec}{\mathbf b}\) \(\newcommand{\cvec}{\mathbf c}\) \(\newcommand{\dvec}{\mathbf d}\) \(\newcommand{\dtil}{\widetilde{\mathbf d}}\) \(\newcommand{\evec}{\mathbf e}\) \(\newcommand{\fvec}{\mathbf f}\) \(\newcommand{\nvec}{\mathbf n}\) \(\newcommand{\pvec}{\mathbf p}\) \(\newcommand{\qvec}{\mathbf q}\) \(\newcommand{\svec}{\mathbf s}\) \(\newcommand{\tvec}{\mathbf t}\) \(\newcommand{\uvec}{\mathbf u}\) \(\newcommand{\vvec}{\mathbf v}\) \(\newcommand{\wvec}{\mathbf w}\) \(\newcommand{\xvec}{\mathbf x}\) \(\newcommand{\yvec}{\mathbf y}\) \(\newcommand{\zvec}{\mathbf z}\) \(\newcommand{\rvec}{\mathbf r}\) \(\newcommand{\mvec}{\mathbf m}\) \(\newcommand{\zerovec}{\mathbf 0}\) \(\newcommand{\onevec}{\mathbf 1}\) \(\newcommand{\real}{\mathbb R}\) \(\newcommand{\twovec}[2]{\left[\begin{array}{r}#1 \\ #2 \end{array}\right]}\) \(\newcommand{\ctwovec}[2]{\left[\begin{array}{c}#1 \\ #2 \end{array}\right]}\) \(\newcommand{\threevec}[3]{\left[\begin{array}{r}#1 \\ #2 \\ #3 \end{array}\right]}\) \(\newcommand{\cthreevec}[3]{\left[\begin{array}{c}#1 \\ #2 \\ #3 \end{array}\right]}\) \(\newcommand{\fourvec}[4]{\left[\begin{array}{r}#1 \\ #2 \\ #3 \\ #4 \end{array}\right]}\) \(\newcommand{\cfourvec}[4]{\left[\begin{array}{c}#1 \\ #2 \\ #3 \\ #4 \end{array}\right]}\) \(\newcommand{\fivevec}[5]{\left[\begin{array}{r}#1 \\ #2 \\ #3 \\ #4 \\ #5 \\ \end{array}\right]}\) \(\newcommand{\cfivevec}[5]{\left[\begin{array}{c}#1 \\ #2 \\ #3 \\ #4 \\ #5 \\ \end{array}\right]}\) \(\newcommand{\mattwo}[4]{\left[\begin{array}{rr}#1 \amp #2 \\ #3 \amp #4 \\ \end{array}\right]}\) \(\newcommand{\laspan}[1]{\text{Span}\{#1\}}\) \(\newcommand{\bcal}{\cal B}\) \(\newcommand{\ccal}{\cal C}\) \(\newcommand{\scal}{\cal S}\) \(\newcommand{\wcal}{\cal W}\) \(\newcommand{\ecal}{\cal E}\) \(\newcommand{\coords}[2]{\left\{#1\right\}_{#2}}\) \(\newcommand{\gray}[1]{\color{gray}{#1}}\) \(\newcommand{\lgray}[1]{\color{lightgray}{#1}}\) \(\newcommand{\rank}{\operatorname{rank}}\) \(\newcommand{\row}{\text{Row}}\) \(\newcommand{\col}{\text{Col}}\) \(\renewcommand{\row}{\text{Row}}\) \(\newcommand{\nul}{\text{Nul}}\) \(\newcommand{\var}{\text{Var}}\) \(\newcommand{\corr}{\text{corr}}\) \(\newcommand{\len}[1]{\left|#1\right|}\) \(\newcommand{\bbar}{\overline{\bvec}}\) \(\newcommand{\bhat}{\widehat{\bvec}}\) \(\newcommand{\bperp}{\bvec^\perp}\) \(\newcommand{\xhat}{\widehat{\xvec}}\) \(\newcommand{\vhat}{\widehat{\vvec}}\) \(\newcommand{\uhat}{\widehat{\uvec}}\) \(\newcommand{\what}{\widehat{\wvec}}\) \(\newcommand{\Sighat}{\widehat{\Sigma}}\) \(\newcommand{\lt}{<}\) \(\newcommand{\gt}{>}\) \(\newcommand{\amp}{&}\) \(\definecolor{fillinmathshade}{gray}{0.9}\)The following set of experiments introduce students to the applications of gravimetry.
- Burrows, H. D.; Ellis, H. A.; Odilora, C. A. “The Dehydrochlorination of PVC,” J. Chem. Educ. 1995, 72, 448–450.
- Carmosini, N.; Ghoreshy, S. Koether, M. C. “The Gravimetric Analysis of Nickel Using a Microwave Oven,” J. Chem. Educ. 1997, 74, 986–987.
- Harris, T. M. “Revitalizing the Gravimetric Determination in Quantitative Analysis Laboratory,” J. Chem. Educ. 1995, 72, 355–356.
- Henrickson, C. H.; Robinson, P. R. “Gravimetric Determination of Calcium as CaC2O4•H2O,” J. Chem. Educ. 1979, 56, 341–342.
- Shaver, L. A. “Determination of Phosphates by the Gravimetric Quimociac Technique,” J. Chem. Educ. 2008, 85, 1097–1098.
- Snow, N. H.; Dunn, M.; Patel, S. “Determination of Crude Fat in Food Products by Supercritical Fluid Extraction and Gravimetric Analysis,” J. Chem. Educ. 1997, 74, 1108–1111.
- Thompson, R. Q.; Ghadiali, M. “Microwave Drying of Precipitates for Gravimetric Analysis,” J. Chem. Educ. 1993, 70, 170–171.
- Wynne, A. M. “The Thermal Decomposition of Urea,” J. Chem. Educ. 1987, 64, 180–182.
The following resources provide a general history of gravimetry.
- A History of Analytical Chemistry; Laitinen, H. A.; Ewing, G. W., Eds.; The Division of Analytical Chemistry of the American Chemical Society: Washington, D. C., 1977, pp. 10–24.
- Beck, C. M. “Classical Analysis: A Look at the Past, Present, and Future,” Anal. Chem. 1991, 63, 993A–1003A; Anal. Chem. 1994, 66, 224A–239A
Consult the following texts for additional examples of inorganic and organic gravimetric methods include the following texts.
- Bassett, J.; Denney, R. C.; Jeffery, G. H.; Mendham, J. Vogel’s Textbook of Quantitative Inorganic Analysis, Longman: London, 4th Ed., 1981.
- Erdey, L. Gravimetric Analysis, Pergamon: Oxford, 1965.
- Steymark, A. Quantitative Organic Microanalysis, The Blakiston Co.: NY, 1951.
- Wendlandt, W. W. Thermal Methods of Analysis, 2nd Ed. Wiley: NY. 1986.
For a review of isotope dilution mass spectrometry see the following article.
- Fassett, J. D.; Paulsen, P. J. “Isotope Dilution Mass Spectrometry for Accurate Elemental Analysis,” Anal. Chem. 1989, 61, 643A–649A.