CHEM 401L: Analytical Chemistry Lab Manual
- Page ID
- 401122
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\(\newcommand{\avec}{\mathbf a}\) \(\newcommand{\bvec}{\mathbf b}\) \(\newcommand{\cvec}{\mathbf c}\) \(\newcommand{\dvec}{\mathbf d}\) \(\newcommand{\dtil}{\widetilde{\mathbf d}}\) \(\newcommand{\evec}{\mathbf e}\) \(\newcommand{\fvec}{\mathbf f}\) \(\newcommand{\nvec}{\mathbf n}\) \(\newcommand{\pvec}{\mathbf p}\) \(\newcommand{\qvec}{\mathbf q}\) \(\newcommand{\svec}{\mathbf s}\) \(\newcommand{\tvec}{\mathbf t}\) \(\newcommand{\uvec}{\mathbf u}\) \(\newcommand{\vvec}{\mathbf v}\) \(\newcommand{\wvec}{\mathbf w}\) \(\newcommand{\xvec}{\mathbf x}\) \(\newcommand{\yvec}{\mathbf y}\) \(\newcommand{\zvec}{\mathbf z}\) \(\newcommand{\rvec}{\mathbf r}\) \(\newcommand{\mvec}{\mathbf m}\) \(\newcommand{\zerovec}{\mathbf 0}\) \(\newcommand{\onevec}{\mathbf 1}\) \(\newcommand{\real}{\mathbb R}\) \(\newcommand{\twovec}[2]{\left[\begin{array}{r}#1 \\ #2 \end{array}\right]}\) \(\newcommand{\ctwovec}[2]{\left[\begin{array}{c}#1 \\ #2 \end{array}\right]}\) \(\newcommand{\threevec}[3]{\left[\begin{array}{r}#1 \\ #2 \\ #3 \end{array}\right]}\) \(\newcommand{\cthreevec}[3]{\left[\begin{array}{c}#1 \\ #2 \\ #3 \end{array}\right]}\) \(\newcommand{\fourvec}[4]{\left[\begin{array}{r}#1 \\ #2 \\ #3 \\ #4 \end{array}\right]}\) \(\newcommand{\cfourvec}[4]{\left[\begin{array}{c}#1 \\ #2 \\ #3 \\ #4 \end{array}\right]}\) \(\newcommand{\fivevec}[5]{\left[\begin{array}{r}#1 \\ #2 \\ #3 \\ #4 \\ #5 \\ \end{array}\right]}\) \(\newcommand{\cfivevec}[5]{\left[\begin{array}{c}#1 \\ #2 \\ #3 \\ #4 \\ #5 \\ \end{array}\right]}\) \(\newcommand{\mattwo}[4]{\left[\begin{array}{rr}#1 \amp #2 \\ #3 \amp #4 \\ \end{array}\right]}\) \(\newcommand{\laspan}[1]{\text{Span}\{#1\}}\) \(\newcommand{\bcal}{\cal B}\) \(\newcommand{\ccal}{\cal C}\) \(\newcommand{\scal}{\cal S}\) \(\newcommand{\wcal}{\cal W}\) \(\newcommand{\ecal}{\cal E}\) \(\newcommand{\coords}[2]{\left\{#1\right\}_{#2}}\) \(\newcommand{\gray}[1]{\color{gray}{#1}}\) \(\newcommand{\lgray}[1]{\color{lightgray}{#1}}\) \(\newcommand{\rank}{\operatorname{rank}}\) \(\newcommand{\row}{\text{Row}}\) \(\newcommand{\col}{\text{Col}}\) \(\renewcommand{\row}{\text{Row}}\) \(\newcommand{\nul}{\text{Nul}}\) \(\newcommand{\var}{\text{Var}}\) \(\newcommand{\corr}{\text{corr}}\) \(\newcommand{\len}[1]{\left|#1\right|}\) \(\newcommand{\bbar}{\overline{\bvec}}\) \(\newcommand{\bhat}{\widehat{\bvec}}\) \(\newcommand{\bperp}{\bvec^\perp}\) \(\newcommand{\xhat}{\widehat{\xvec}}\) \(\newcommand{\vhat}{\widehat{\vvec}}\) \(\newcommand{\uhat}{\widehat{\uvec}}\) \(\newcommand{\what}{\widehat{\wvec}}\) \(\newcommand{\Sighat}{\widehat{\Sigma}}\) \(\newcommand{\lt}{<}\) \(\newcommand{\gt}{>}\) \(\newcommand{\amp}{&}\) \(\definecolor{fillinmathshade}{gray}{0.9}\)This manual is the culmination of the efforts of many individuals. While some of the experiments are "classics", and appear in various forms in many Quantitative Analysis textbooks and laboratory manuals, much effort was expended to ensure that the experiments work well here at Duke and thus each experiment has been extensively tailored for our laboratory program. We view this manual as one of continual modification, and often improvements arise from comments and criticisms. We thus encourage you to discuss ideas for improvements with your TA and instructor.
- 5: Determination of cocaine on bills using Gas Chromatography, Mass Spectrometry (GC-MS)
- 5.1: GC-MS Pre-lab Assignment
- 5.2: Introduction to Gas Chromatography Instrumentation
- 5.3: Quantitative and Qualitative GC and GC-MS
- 5.4: Mass Spectrometers
- 5.5: Interpreting Electron Ionization Mass Spectra
- 5.6: GC-MS Procedure and instructions for data analysis
- 5.7: GC-MS Instruments at Duke
- 5.8: Instructions for Operating the Agilent 7820A/5975 GCMS
- 5.9: Instructions for Data Processing using MSD ChemStation Data Analysis Software
- 5.10: TA Notes
- 5.11: Data Analysis using Agilent Mass Hunter Quantitative Analysis
- 5.12: Data Analysis with Agilent Mass Hunter Qualitative Software
- 6: Determination of metals using Inductively coupled plasma, optical emission spectroscopy (ICP-OES)
- 6.1: Pre-Lab assignment
- 6.2: Atomic Emission Spectroscopy
- 6.3: ICP-OES Procedure and instructions for treatment of data
- 6.4: ICP-OES Instrument at Duke
- 6.5: Writing a method for the Perkin Elmer Avio 220 Max
- 6.6: ICP-OES Operation Instructions
- 6.7: Instructions for Viewing and Exporting Data using Syngistics Software
- 6.8: TA Notes
Contributors and Attributions
- W. R. Fawcett, John Berg, P. B. Kelley, Carlito B. Lebrilla, Gang-yu Liu, Delmar Larsen, Paul Hrvatin, David Goodin, and Brooke McMahon
- https://chem.libretexts.org/Courses/..._-_Lab_Manual#
- Kathryn Haas, Todd Woerner