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Chemistry LibreTexts

1.2: Glassware and Equipment

  • Page ID
    93163
    • 1.2A: Pictures of Glassware and Equipment
    • 1.2B: Ground Glass Joints
      Most organic glassware uses "ground glass joints," which have a frosted appearance. They are precisely ground to a certain size (which makes them expensive) and have outer (female) and inner (male) joints so that pieces can be connected together with a tight fit. Common joint sizes are 14/20, 19/22, and 24/40. The first number refers to the inner diameter (in millimeters) of a female joint or outer diameter of a male joint. The second number refers to the length of the joint.
    • 1.2C: Clamping
      Metal clamps are used to connect glassware to ring stands or the metal lattice work. Two common type of clamps are "extension clamps" and "three-fingered clamps". Although in many situations the clamps can be used interchangeably, an extension clamp must be used when clamping to a round bottomed flask as 3-fingered clamps do not hold well.
    • 1.2D: Greasing Joints
      Ground glass joints are manufactured to fit quite well with one another, and yet they are not perfectly airtight. In some situations (e.g. when using reduced pressure inside an apparatus), grease must be applied to each joint to ensure a good seal. Grease is also used whenever the joint may be in contact with a highly basic solution, as basic solutions can form sodium silicates and etch glass.
    • 1.2E: Cleaning Glassware
      Glassware should be dismantled and cleaned as soon as possible. Experience with home dishwashing can tell you that dishes are more difficult to clean when allowed to dry. If there is a time constraint, it's best to leave glassware in a tub of soapy water.
    • 1.2F: Drying Glassware
      Glassware that appears "dry" actually contains a thin film of water condensation on its surface. When using reagents that react with water (sometimes violently!), this water layer needs to be removed.
    • 1.2G: 1.1G- Storing Samples (Parafilm

    Contributor

    Lisa Nichols (Butte Community College). Organic Chemistry Laboratory Techniques is licensed under a Creative Commons Attribution-NonCommercial-NoDerivatives 4.0 International License. Complete text is available online.

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