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Chemistry LibreTexts

8.5 Problem 4

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Learning Objectives
  • Determine the structure for the following problem.
Exercise 1

Solve the structure using the following spectral data. 

Mass Spectrum:

clipboard_e92ac0b9889f1b4fc70ee52ae8fdaa3fb.png

13C Spectrum:

clipboard_e25e7a8fc8efb338e74f2f135fed99ac3.png

DEPT-135 Spectrum: 

clipboard_e8d0b1f19491bdd9187a7ff10ffeb2692.png

1H NMR Spectrum:

Integration: 1:1:1:1:3:9

clipboard_ef0b88e4b7f0376c5e74f0551b1486df5.png

1H NMR Spectrum Zoomed in from 7 ppm to 8.3 ppm:

clipboard_e19e2ffdaa59cb63fac96ba15860f2e01.png

COSY: 

clipboard_e108b5c801ab3ee0316796dc695c6ec2b.png

HSQC: 

clipboard_e80ba32902004b8f122d9a2397eeb1d5f.png

Answer

FinalProblem4.svg

 

 


8.5 Problem 4 is shared under a not declared license and was authored, remixed, and/or curated by Lauren Reutenauer.

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