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Vacuum Filtration

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    21654
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    Suction filtration is a chemistry laboratory technique which allows for a greater rate of filtration. Whereas in normal filtration gravity provides the force which draws the liquid through the filter paper, in suction filtration a pressure gradient performs this function. This has the advantage of offering a variable rate depending on the strength of the pump being used to extract air from the Büchner flask. Care must be taken not to use such a strong vacuum that the filter paper rips (in which case all the solid will be lost back into the solvent) or in extreme cases the glass flask breaks. Suction filtration is used in recrystallisation experiments.

    Diagram of a vacuum filtration setup. A Buchner funnel with moistened filter paper placed atop a porous plate is placed into a Buchner flask and secured with a rubber bung. Rubber tubing connects the Buchner flask to an aspirator to create a partial vacuum within the flask.

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