7.1: Learning Objectives
- Page ID
- 212929
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This experiment is intended to illustrate the following concepts and techniques:
• Heating under reflux
• Theory, technique, and use of simple distillation
• Boiling point determination techniques
• Microscale assembly of a simple distillation apparatus
This manuscript will refer you to the following pages and figures from your textbook. You may want to mark them beforehand.
- p. 600 – 603, section 7.2 and the following figures:
- Fig. 7.6 – Reflux apparatus
- Fig. 7.7 – Reflux ring
- Fig. 7.8B – Microscale magnetic spin vane
• p. 694 – 696, section 13.1 and 13.2 and the following figure:
- Fig. 13.3 – Macroscale method of determining the boiling point
• p. 703 – 710, and the following figures:
- Fig. 14.2 – Three types of temperature behaviour during a simple distillation
- Fig. 14.4 – The Hickman head
- Fig. 14.5 – Microscale distillation apparatus
- Fig. 14.6 – Removing the distillate from the Hickman head
• p. 103 – 108 (exp. 13)