9.1: Purpose of the Experiment
- Page ID
- 212003
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I. Purpose of the Experiment
This is an integrated experiment, which combines techniques from Organic, Thermodynamics, Physical, and Analytical chemistry. It has been designed to introduce the student to:
- Organic Synthesis: Synthesizing an ester from an acid catalyzed reaction of a carboxylic acid and alcohol
- Fundamental Chemical Engineering Separation Process principles on refluxing
- Two phase solvent extraction using a Separatory Funnel
- Distillation at atmospheric pressure
- Precise handling and measurement techniques for volatile organic liquids
- Correct handling and operation of a Mass Spectrometer & NMR Spectrometer
- Thermodynamics, solution chemistry, intermolecular bonding, and organic nomenclature